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ACQUITY UPLC方法验证系统包

更新时间:2021-01-12

简要描述:

ACQUITY UPLC方法验证系统包
提供三批色谱填料(来自不同批次的颗粒基体)以判断一个分析方法的耐受性,可靠性和一致性。

ACQUITY UPLC方法验证系统包

UPLC方法验证包— 确保方法耐用性

 

 

为了确保分析方法持续可靠且具有重现性,采用多批色谱填料进行检测和验证变得尤为重要。作为硅胶杂化颗粒的主要生产商,沃特世公司为不同批次之间的重现性设立了行业的基准。基于信誉*的颗粒和色谱柱生产的过程控制,使批与批和柱与柱之间的变异性小化,从而为分析方法长期的可靠性提供信心。

 

ACQUITY UPLC方法验证包提供三批色谱填料(来自不同批次的颗粒基体)以判断一个分析方法的耐受性,可靠性和一致性。

来自三个不同批次的填料基体的三个不同批次的键合处理的ACQUITY UPLC柱对氯氨平有关物质的分析表现出zhuo越的重现性,保证了分析方法的长期重现性。

选择性(a)
批号杂质C杂质A氯氨平杂质B
1191.031.071.071.59
1201.031.071.071.58
1241.021.071.071.58

 

 

ACQUITY UPLC方法验证系统包

订货信息:

ACQUITY UPLC方法开发套装[MDK: Method Development Kit]

套装名称数量固定相颗粒大小配置部件编号
选择性*大化大化UPLC方法开发套装:宽泛的选择性用于方法开发,包括在低pH和高pH下。是低离子强度添加剂条件时(例如甲酸)的*佳佳选择
选择性*大化UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176002123
选择性*大化UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176002124
选择性*大化UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176002125
选择性*大化UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, HSS C18 SBCSH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176002126
高&低pH,宽选择性的UPLC色谱柱套装:通过开拓低和高流动相pH使分离选择性宽
高&低pH,宽选择性的UPLC色谱柱套装4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm2.1 x 50 mm176001042
高&低pH,宽选择性的UPLC色谱柱套装4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm2.1 x 100 mm176001043
高&低pH,宽选择性的UPLC色谱柱套装4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm3.0 x 50 mm176001881
高&低pH,宽选择性的UPLC色谱柱套装4件/包BEH C18, BEH C8, BEH Shield RP18,   BEH苯基BEH 1.7 μm3.0 x 100 mm176001882
UPLC方法开发套装:通过开拓低和高流动相pH(BEH色谱柱)将分离选择性*大化大化和适用于极性化合物保留性(HSS   T3)
UPLC方法开发套装4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001603
UPLC方法开发套装4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001604
UPLC方法开发套装4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001883
UPLC方法开发套装4件/包BEH C18, BEH Shield RP18, BEH 苯基, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001884
L1   UPLC色谱柱套装:依从USP药典中L1类别,但提供不同硅醇基活性和疏水性的C18色谱柱
L1 UPLC色谱柱套装4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001605
L1 UPLC色谱柱套装4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001606
L1 UPLC色谱柱套装4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001885
L1 UPLC色谱柱套装4件/包BEH C18, BEH Shield RP18, HSS C18, HSS   T3BEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001886
质谱UPLC色谱柱套装:直链烷烃C18柱,具有不同的硅醇活性、峰形、选择性和疏水性,且无MS流失问题
质谱UPLC色谱柱套装4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001607
质谱UPLC色谱柱套装4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001608
质谱UPLC色谱柱套装4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001887
质谱UPLC色谱柱套装4件/包BEH C18, HSS C18, HSS T3, HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001888
低pH,宽选择性UPLC色谱柱套装:有各种不同的键合相和选择性,用于开发低pH流动相条件下的反相方法
低pH,宽选择性UPLC色谱柱套装4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001609
低pH,宽选择性UPLC色谱柱套装4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001610
低pH,宽选择性UPLC色谱柱套装4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001889
低pH,宽选择性UPLC色谱柱套装4件/包BEH Shield RP18, BEH 苯基, HSS C18, HSS   C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001890
选择性*大化大化的RP 和 HILIC   UPLC方法开发套装:通过综合HILIC和RP固定相以提供宽分离选择性,用以保留分离跨越宽泛极性范围的分析物
选择性*大化的RP 和   HILIC UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm2.1 x 50 mm176002127
选择性*大化的RP 和   HILIC UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm2.1 x 100 mm176002128
选择性*大化的RP 和   HILIC UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm3.0 x 50 mm176002129
选择性*大化的RP 和   HILIC UPLC方法开发套装4件/包CSH C18, CSH苯己基, CSH氟苯基, BEH AmideCSH 1.7 μm; BEH 1.7 μm3.0 x 100 mm176002130
UPLC   RP和HILIC方法开发套装:通过综合RP和HILIC固定相以提供宽分离选择性,用以保留分离跨越宽泛极性范围的分析物
UPLC RP和HILIC   方法开发套装4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 50 mm176001959
UPLC RP和HILIC   方法开发套装4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm2.1 x 100 mm176001960
UPLC RP和HILIC   方法开发套装4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 50 mm176001961
UPLC RP和HILIC   方法开发套装4件/包BEH C18, BEH Shield RP18, BEH Amide,   HSS C18 SBBEH 1.7 μm; HSS 1.8 μm3.0 x 100 mm176001962
UPLCHILIC方法开发套装:在低pH(对碱性分析物)和高pH(对酸性分析物)下为极性和/或可离子化化合物轻松开发HILIC方法
UPLCHILIC方法开发套装4件/包BEH Amide, BEH HILICBEH 1.7 μm2.1 x 50 mm176001963
UPLCHILIC方法开发套装4件/包BEH Amide, BEH HILICBEH 1.7 μm2.1 x 100 mm176001964
UPLCHILIC方法开发套装4件/包BEH Amide, BEH HILICBEH 1.7 μm3.0 x 50 mm176001965
UPLCHILIC方法开发套装4件/包BEH Amide, BEH HILICBEH 1.7 μm3.0 x 100 mm176001966

 

 

ACQUITY UPLC方法转换套装[MTK: Method Transfer Kit]*

套装名称UPLC Column 2.1 mm IDHPLC Column 4.6 mm ID部件编号
CSH C18 1.7 to   5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186005529
CSH   Phenyl-Hexyl 1.7 to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186005530
CSH   Fluoro-Phenyl 1.7 to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186005531
BEH C18 1.7 to   5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186004958
BEH Shield   RP18 1.7 to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186004959
BEH HILIC 1.7   to 5 μm MTK50 mm, 1.7 μm150 mm, 5 μm186004960
HSS C18 1.8 to   5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186004961
HSS T3 1.8 to   5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186004962
HSS C18 SB 1.8   to 5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186004963
HSS Cya.8   to 5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186005979
HSS PFP 1.8 to   5 μm MTK50 mm, 1.8 μm150 mm, 5 μm186006000
CSH C18 1.7 to   3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186005532
CSH   Phenyl-Hexyl 1.7 to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186005533
CSH   Fluoro-Phenyl 1.7 to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186005534
BEH C18 1.7 to   3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004964
BEH Shield   RP18 1.7 to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004965
BEH HILIC 1.7   to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004966
BEH Amide 1.7   to 3.5 μm MTK50 mm, 1.7 μm100 mm, 3.5 μm186004967
HSS C18 1.8 to   3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186004968
HSS T3 1.8 to   3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186004969
HSS C18 SB 1.8   to 3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186004970
HSS Cya.8   to 3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186005980
HSS PFP 1.8 to   3.5 μm MTK50 mm, 1.8 μm100 mm, 3.5 μm186006001
CSH C18 1.7 to   3.5 μm High Rs MTK100 mm, 1.7 μm150 mm, 3.5 μm186005535
CSH   Phenyl-Hexyl 1.7 to 3.5 μm高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186005536
CSH   Fluoro-Phenyl 1.7 to 3.5 μm高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186005537
BEH C18 1.7 to   3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004971
BEH Shield   RP18 1.7 to 3.5 μm高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004972
BEH HILIC 1.7   to 3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004973
BEH Amide 1.7   to 3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004974
HSS C18 1.8 to   3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004975
HSS T3 1.8 to   3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004976
HSS C18 SB 1.8   to 3.5 μm 高分辨 MTK100 mm, 1.7 μm150 mm, 3.5 μm186004977
HSS Cya.8   to 3.5 μm 高分辨 MTK100 mm, 1.8 μm150 mm, 3.5 μm186005981
HSS PFP 1.8 to   3.5 μm 高分辨 MTK100 mm, 1.8 μm150 mm, 3.5 μm186006002

*每个套装都含有一根UPLC色谱柱和一根HPLC色谱柱,可从ACQUITY UPLC在线社区
www.waters。。com/myuplc下载ACQUITY UPLC Columns Calculator用于计算方法转移。

 

 

ACQUITY UPLC方法验证套装[MVK:Method Validation Kit]**

固定相粒径色谱柱长度部件编号 2.1 mm ID部件编号 3.0 mm ID
CSH C181.7 μm50 mm186005571186005573
CSH C181.7 μm100 mm186005572186005574
CSH 苯己基1.7 μm50 mm186005579186005581
CSH 苯己基1.7 μm100 mm186005580186005582
CSH 氟苯基1.7 μm50 mm186005575186005577
CSH 氟苯基1.7 μm100 mm186005576186005578
BEH C181.7 μm50 mm186004044186004691
BEH C181.7 μm100 mm186004045186004692
BEH C81.7 μm50 mm186004046186004693
BEH C81.7 μm100 mm186004047186004694
BEH Shield   RP181.7 μm50 mm186004048186004695
BEH Shield   RP181.7 μm100 mm186004049186004696
BEH Phenyl1.7 μm50 mm186004050186004697
BEH Phenyl1.7 μm100 mm186004052186004698
BEH HILIC1.7 μm50 mm186004053186004699
BEH HILIC1.7 μm100 mm186004054186004700
BEH Amide1.7 μm50 mm186004807186004809
BEH Amide1.7 μm100 mm186004808186004810
BEH130 C181.7 μm100 mm186004896-
BEH300 C181.7 μm100 mm186004897-
BEH300 C41.7 μm100 mm186004899-
寡核苷酸 C181.7 μm100 mm186004898-
Glycan BEH   Amide1.7 μm100 mm186004907-
HSS T31.8 μm50 mm186004055186004701
HSS T31.8 μm100 mm186004056186004702
HSS C181.8 μm50 mm186004057186004703
HSS C181.8 μm100 mm186004058186004704
HSS C 18 SB1.8 μm50 mm186004137186004705
HSS C 18 SB1.8 μm100 mm186004138186004709
HSS PFP1.8 μm50 mm186005975-
HSS PFP1.8 μm100 mm186005976-
HSS PFP1.8 μm50 mm186005977-
HSS PFP1.8 μm100 mm186005978-
HSS 氰基1.8 μm50 mm186005996186005998
HSS 氰基1.8 μm100 mm186005997186005999

**每个套装包括来自3个不同批次填料的3根色谱柱。

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